HuagongsheHuagongshe Chemistry Print Report · For research reference only
19967-22-7 → HCID 19745920, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 19967-22-7 | HCID 14266244 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 19745920 | HCID 19745920 | — |
Reaction Steps
To a suspension of pyridinium chlorochromate (PCC) (5 g) in CH2Cl2 (200 mL) and 4 angstrom molecule sieves (5 g) was added the alcohol (2 g) (Step II). The mixture was stirred 2 hr at RT, filtered through celite and evaporated. Flash chromatography using 25% ethyl acetate in hexane afforded the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05232916 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-87a7ecd7861b41da8240b4e00a100531 |
| Source note | uspto-grants-1993_08 |