HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromomethylnaphthalene → 4-Methoxy-2,2-dimethyl-4-[3-(naphth-2-ylmethoxy)phenyl]tetrahydropyran
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromomethylnaphthalene | HCID 70320 | — |
| Reactant | 4-(3-Hydroxyphenyl)-4-methoxy-2,2-dimethyltetrahydropyran | HCID 20080655 | — |
| Product | 4-Methoxy-2,2-dimethyl-4-[3-(naphth-2-ylmethoxy)phenyl]tetrahydropyran | HCID 20080590 | 95.4% |
Reaction Steps
Using the procedure described in Example 5, 2-bromomethylnaphthalene (0.245 g) was reacted with 4-(3-hydroxyphenyl)-4-methoxy-2,2-dimethyltetrahydropyran (0.25 g) to give 4-methoxy-2,2-dimethyl-4-[3-(naphth-2-ylmethoxy)phenyl]tetrahydropyran (0.38 g, 95%), as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05234950 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-7dc9171de1dd48ee9576080151df0442 |
| Source note | uspto-grants-1993_08 |