HuagongsheHuagongshe Chemistry Print Report · For research reference only
methyl (2R)-2-amino-3-phenylpropanoate;hydrochloride → HCID 22846354, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | methyl (2R)-2-amino-3-phenylpropanoate;hydrochloride | HCID 11481330 | — |
| Reactant | HCID 22846355 | HCID 22846355 | — |
| Solvent | Ethylacetate methanol | HCID 21584119 | — |
| Product | HCID 22846354 | HCID 22846354 | — |
Reaction Steps
The procedure of Example 12 (ii-iii) was followed using D-phenylalanine methyl ester hydrochloride in place lycine methyl ester hydrochloride. The intermediate N-[{2-n-butyl-1-(2-chlorophenyl)methyl-1H-imidazol-5 -yl}methylcarbonyl]-D-phenylalanine methyl ester was a solid; mp 179°-181° C. (from methanol/ethyl acetate). The title compound was a solid; mp 178°-181° C. (from methanol/ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05234917 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-66e0d1efe54246a99f77e61522682c32 |
| Source note | uspto-grants-1993_08 |