Hydrogen Peroxide → HCID 53664281, compound

Participants

Reaction Conditions

Reaction Steps

31.6 g (0.1 mol) of N-phenylcarbamoyllaurolactam are dissolved in 50.0 g of methanesulfonic acid (98% strength by weight), 3.6 g (0.2 mol) of water are added and the mixture is heated at 80° C. for 30 minutes. After cooling the reaction mixture to 25° C., 17.0 g (0.25 mol) of hydrogen peroxide (50% strength by weight) are added dropwise such that the internal temperature can be kept between 22 and 25° C. After stirring at 25° C. for 20 minutes, 100 ml of water are added and the precipitated peroxycarboxylic acid is filtered off with suction. The filter cake is washed free of mineral acid with water and dried at 40° C. in a water pump vacuum.

Provenance & Evidence