HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroquinone → HCID 67763450, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroquinone | HCID 785 | — |
| Reactant | Phenylacetyl chloride | HCID 7679 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | 1,1-Dichloroethane | HCID 6365 | — |
| Product | HCID 67763450 | HCID 67763450 | 23.7% |
Reaction Steps
22 g (0.2 mole) of hydroquinone were dissolved in 60 ml of dichloroethane and 26.8 g (0.2 mole) of anhydrous aluminum chloride were added to the solution. To the obtained complex 30.8 g (0.2 mole) of phenyl-acetyl chloride in 30 ml of dichloroethane were added. Further the procedure of Example 1 was followed. 10.1 g of 2,5-dihydroxy-phenyl-benzyl-ketone were obtained, m.p.: 118°-120° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05235109 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-b119d74654504b288f84c82441a0c814 |
| Source note | uspto-grants-1993_08 |