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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2254396Generated: October 30, 2026

1-Octanol → HCID 19745022, compound

https://huagongshe.com/reaction/2254396

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1-OctanolHCID 957—
ReactantMethanesulfonic AcidHCID 6395—
ReactantHCID 19745021HCID 19745021—
ProductHCID 19745022HCID 1974502232.5%

Reaction Steps

The general procedure of Example 12 is repeated using 10.0 g (0.035 mole) 1-hydroxy-2,6-diphenyl-4-piperidone oxime, 25.0 g (0.19 moles) 1-octanol and 7.0 g (0.073 moles) methanesulfonic acid. 5.8 g (32% yield) of the title compound is isolated as a clear oil after purification by LC (silica gel, ethyl acetate:hexane).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05235056
Source datasetuspto-grants-1993_08
ORD IDord-1afda0375e7b43de9063f31cbb6e9616
Source noteuspto-grants-1993_08