HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(p-cyanophenylmethyl)-5-(2-formylethyl)-1H-imidazole → 5-(p-Cyanophenyl)-7,8-dihydroimidazo[1,5-a]pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(p-cyanophenylmethyl)-5-(2-formylethyl)-1H-imidazole | HCID 15294731 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 5-(p-Cyanophenyl)-7,8-dihydroimidazo[1,5-a]pyridine | HCID 15294718 | — |
Reaction Steps
A solution of 0.24 g of 1-(p-cyanophenylmethyl)-5-(2-formylethyl)-1H-imidazole in 10 ml of anhydrous ethanol is refluxed under nitrogen for 2 h with 20 mg of potassium tert-butoxide, cooled and evaporated to yield the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05428160 |
| Source dataset | uspto-grants-1995_06 |
| ORD ID | ord-25456296e8c146dfafa23125ee1642c6 |
| Source note | uspto-grants-1995_06 |