HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 53965818, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 19744829 | HCID 19744829 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53965818 | HCID 53965818 | 92% |
Reaction Steps
170 mg of the aldehyde compound was dissolved in 20 ml of ethanol, and 100 mg of sodium borohydride was added. The mixture was stirred at room temperature for 1 hour. Water and ethyl ether were added to the reaction mixture to dilute it, and it was then worked up in a customary manner to give 158 mg (yield 92%) of 3-(3-methyl-2-butenyl)benzyl alcohol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05234946 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-b625c86e24634219a60d5ebf54e787ac |
| Source note | uspto-grants-1993_08 |