HRID2254439

反应详情

EQUATION

反应方程式

HRID 2254439 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Ethyl 3-(2-furyl)benzoate J. Chem. Soc., (B), 1971, 2305] was dissolved in 5 ml of anhydrous ethyl ether, and with stirring under ice cooling, 23 mg of lithium aluminum hydride was added. The mixture was stirred for 40 minutes. After the reaction, the reaction mixture was extracted by adding water and ethyl ether. The extract was worked up in a customary manner to give 170 mg (yield 83%) of 3-(2-furyl)benzyl alcohol.

WORKUP

后处理

  1. stirringThe mixture was stirred for 40 minutes
  2. customAfter the reaction
  3. extractionthe reaction mixture was extracted
  4. additionby adding water and ethyl ether