反应详情

160 mg of the resulting alcohol compound was dissolved in 3 ml of anhydrous ethyl ether. Thionyl chloride (73 microliters) was added, and under ice cooling, the mixture was stirred for 3 hours. After the reaction, the reaction mixture was washed with a saturated aqueous solution of sodium chloride and 5% sodium hydrogen carbonate to give an ethyl ether solution of the captioned compound. It was used directly in the reaction of Example 58.

1. customAfter the reaction
2. washthe reaction mixture was washed with a saturated aqueous solution of sodium chloride and 5% sodium hydrogen carbonate
3. customto give an ethyl ether solution of the captioned compound
4. customIt was used directly in the reaction of Example 58