HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → HCID 19744721, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | HCID 21186163 | HCID 21186163 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 19744721 | HCID 19744721 | 66.5% |
Reaction Steps
2.40 g of 3-(3-thienyl)benzyl chloride was dissolved in 40 ml of toluene, and 3.62 g of triphenylphosphine was added. The mixture was heated under reflux for 50 hours. The reaction mixture was allowed to cool, and the precipitated crystals were collected by filtration to give 3.60 g (yield 66%) of 3-(3-thienyl)benzyltriphenylphosphonium chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05234946 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-d2acf5356dbd4e5590b5653a732a0b01 |
| Source note | uspto-grants-1993_08 |