HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-bromobutanimide → HCID 19744480, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | Ethyl 5-methylisoxazole-3-carboxylate | HCID 76677 | — |
| Reactant | HCID 10909912 | HCID 10909912 | — |
| Reactant | HCID 19744650 | HCID 19744650 | — |
| Reactant | HCID 19744842 | HCID 19744842 | — |
| Product | HCID 19744480 | HCID 19744480 | — |
Reaction Steps
The same reaction as in Referential Example 49 is carried out except that instead of the starting (E)-N-(6,6-dimethyl-2-hepten-4-ynyl)-N-methyl-4-ethoxycarbonyl-2-pyridylmethylamine, (E)-N-(6,6-dimethyl-2-hepten-4-ynyl)-N-ethyl-3-ethoxycarbonyl-5-isoxazolylmethylamine [synthesized by brominating ethyl 5-methylisoxazole-3-carboxylate with N-bromosuccinimide and condensing the brominated product with (E)-N-ethyl-6,6-dimethyl-2-hepten-4-ynylamine] is used, (E)-N-(6,6-dimethyl-2-hepten-4-ynyl)-N-ethyl-3-formyl-5-isoxazolylamine is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05234946 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-fc8089837db44d52b254713d6e2cde22 |
| Source note | uspto-grants-1993_08 |