HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloromethyl Methyl Ether → HCID 19744652, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloromethyl Methyl Ether | HCID 7864 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2,3-Dihydroxybenzaldehyde | HCID 90579 | — |
| Reactant | HCID 12397048 | HCID 12397048 | — |
| Reactant | HCID 19744759 | HCID 19744759 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 19744652 | HCID 19744652 | — |
Reaction Steps
When 2,3-dihydroxybenzaldehyde is used instead of the starting 3,4-dihydroxybenzaldehyde, and selectively alkylated with methoxymethyl chloride and triethylamine in chloroform to synthesize 3-hydroxy-2-methoxymethyloxybenzaldehyde and thereafter the same reaction as in Referential Example 50 is carried out, (E)-N-(6,6-dimethyl-2-hepten-4-ynyl)-N-methyl-3-hydroxy-2-methoxymethyloxybenzylamine is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05234946 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-715ecdc45bec4ecd907745181b414428 |
| Source note | uspto-grants-1993_08 |