HCID 19744647, compound → HCID 54140041, compound

HRID 2254482Notes

Reaction equation

HRID 2254482 reaction equation
[H-].[Al+3].[Li+].[H-].[H-].[H-].[S:7]1[CH2:12][CH2:11][CH2:10][CH:9]([C:13]2[CH:14]=[C:15]([CH:18]=[CH:19][CH:20]=2)[CH:16]=[O:17])[CH2:8]1>>[S:7]1[CH2:12][CH2:11][CH2:10][CH:9]([C:13]2[CH:14]=[C:15]([CH:18]=[CH:19][CH:20]=2)[CH2:16][OH:17])[CH2:8]1

Participants

3

Reactant 2

HCID 19744647HCID 19744647, compoundHCID 21226445Aluminium lithium hydride

Product 1

HCID 54140041HCID 54140041, compoundYield 14%

Procedure

Using lithium aluminium hydride, the resulting aldehyde compound was reduced in a customary manner to give 75 mg (yield 14%) of the captioned compound as a colorless oil.

Sources & evidence

ORD record
ord-90e1dbd37bd643968fe91ce81bb18c53
Source dataset
uspto-grants-1993_08
Patent number
US05234946

Reaction notes

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