HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Bromomethyl)benzaldehyde → HCID 19744748, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Bromomethyl)benzaldehyde | HCID 7127825 | — |
| Reactant | Stannane, tributyl-3-thienyl- | HCID 10959689 | — |
| Reactant | HCID 19744634 | HCID 19744634 | — |
| Reactant | HCID 19744744 | HCID 19744744 | — |
| Catalyst | HCID 178418397 | HCID 178418397 | — |
| Product | HCID 19744748 | HCID 19744748 | — |
Reaction Steps
Using 3-(4-bromothienylthiomethyl)benzaldehyde [obtained by performing the same reaction as in Referential Example 56 using 4-bromo-2-thiophenethiol [Chem. Abst., 56, 4277 (1962)] and 3-bromomethylbenzaldehyde as starting materials], tributyl(3-thienyl)stannane and tetrakis(triphenylphosphine)palladium, the same reaction as in Referential Example 37 is carried out to give the captioned compound as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05234946 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-db458107c5da44daba5779587d7f51f1 |
| Source note | uspto-grants-1993_08 |