HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → 1-Butyryloxy-2-[p-(p-n-octylphenyl)-benzoyloxy]-propane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Butanoic acid, 2-hydroxypropyl ester | HCID 122419 | — |
| Reactant | 4'-Octyl-4-biphenylcarboxylic acid chloride | HCID 14745967 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 1-Butyryloxy-2-[p-(p-n-octylphenyl)-benzoyloxy]-propane | HCID 19742468 | — |
Reaction Steps
0.75 g of optically active 1-butyryloxy-2-propanol [obtainable by esterification of (S)-1,2-propanediol], 1,7 g of p-(p-n-octylphenyl)-benzoic acid chloride, 20 ml of toluene and 2,1 ml of pyridine are boiled under reflux for 6 hours. The pyridinium chloride is filtered off hot with suction and the filtrate is worked up in the customary manner. Optically active 1-butyryloxy-2-[p-(p-n-octylphenyl)-benzoyloxy]-propane is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05236618 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-a7aae046159c4dd39e1733124b428476 |
| Source note | uspto-grants-1993_08 |