2,5-Dimethyl-1,3-benzoselenazole → HCID 13774191, compound

Participants

Reaction Conditions

Reaction Steps

Into a sealed tube in which air was replaced by nitrogen were placed 1.50 g (7.14 mmoles) of 2,5-dimethylbenzoselenazole and 3.50 g (7.85 mmoles) of octadecyl parachlorobenzenesulfonate. The mixture obtained was heated at 130° C. for 3 hours. The resulting red solid was washed with ether and dried under reduced pressure, giving 2.69 g (yield: 57.4%) of 2,5-dimethyl-3-octadecylbenzoselenazolium parachlorobenzenesulfonate as a light brown powder.

Provenance & Evidence