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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2254837Generated: November 1, 2026

Dichloromethane → HCID 54324550, compound

https://huagongshe.com/reaction/2254837

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDichloromethaneHCID 6344—
Reactant2-(Hydroxyimino)-2-phenylacetonitrileHCID 69998—
ReactantHCID 19708531HCID 19708531—
SolventTriethylamineHCID 8471—
ProductHCID 54324550HCID 5432455093.8%

Reaction Steps

From a mixture of 1.26 g of 2-hydroxyimino-2-phenylacetonitrile, 2.91 g of 9,10-dimethoxyanthracene-2-sulfonyl chloride, 50 ml of dichloromethane, and 0.87 g of triethylamine was obtained 3.61 g of a yellow solid product by the same procedures as in Example 1. The light irradiation was carried out on this compound in the same way as in Example 1, and the leuco dye of the above formula (VI) was added. The compound became a brilliant blue color, and the generation of an acid was observed.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05237059
Source datasetuspto-grants-1993_08
ORD IDord-b1574a27c37642dc832a4db0930adb06
Source noteuspto-grants-1993_08