HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 54324550, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | 2-(Hydroxyimino)-2-phenylacetonitrile | HCID 69998 | — |
| Reactant | HCID 19708531 | HCID 19708531 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 54324550 | HCID 54324550 | 93.8% |
Reaction Steps
From a mixture of 1.26 g of 2-hydroxyimino-2-phenylacetonitrile, 2.91 g of 9,10-dimethoxyanthracene-2-sulfonyl chloride, 50 ml of dichloromethane, and 0.87 g of triethylamine was obtained 3.61 g of a yellow solid product by the same procedures as in Example 1. The light irradiation was carried out on this compound in the same way as in Example 1, and the leuco dye of the above formula (VI) was added. The compound became a brilliant blue color, and the generation of an acid was observed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05237059 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-b1574a27c37642dc832a4db0930adb06 |
| Source note | uspto-grants-1993_08 |