HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 14210546, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-(Bromomethyl)-5-methyl-1,3-dioxol-2-one | HCID 10774141 | — |
| Reactant | HCID 67883991 | HCID 67883991 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 14210546 | HCID 14210546 | — |
Reaction Steps
6.3 g of pyridine-2,4-dicarboxylic acid sodium salt are boiled under reflux with 14.3 g of 5-methyl-2-oxo-1,3-dioxol-4-yl-methyl bromide and 4.5 g of potassium carbonate in 125 ml of dry acetone for 40 hours. The carbonate is filtered off and the solution is chromatographed over silica gel with a 4:1 mixture of toluene and ethyl acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05238948 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-0cadf3e6f1814d978d500eae98b97179 |
| Source note | uspto-grants-1993_08 |