Glycol monoethyl ether → HCID 53655755, compound

HRID 2255075Notes

Reaction equation

HRID 2255075 reaction equation
[N:1]1[CH:6]=[CH:5][C:4]([C:7]([OH:9])=[O:8])=[CH:3][C:2]=1[C:10]([OH:12])=[O:11].[CH2:13]([O:15][CH2:16][CH2:17]O)[CH3:14]>>[N:1]1[CH:6]=[CH:5][C:4]([C:7]([O:9][CH2:14][CH2:13][O:15][CH2:16][CH3:17])=[O:8])=[CH:3][C:2]=1[C:10]([O:12][CH2:17][CH2:16][O:15][CH2:13][CH3:14])=[O:11]

Participants

3

Reactant 2

HCID 8076Glycol monoethyl etherHCID 103652,4-Pyridinedicarboxylic acid

Product 1

HCID 53655755HCID 53655755, compound

Procedure

As described in Example 26, 10 g of pyridine-2,4-dicarboxylic acid are reacted with ethylene glycol monoethyl ether via the acid chloride. The reaction mixture is worked up analogously to Example 26. The product is obtained as an oil. Yield 7.2 g

Workup

  1. customThe product is obtained as an oil

Sources & evidence

ORD record
ord-86f73afa962c4ca9ad9ae206bd228f34
Source dataset
uspto-grants-1993_08
Patent number
US05238948

Reaction notes

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