HuagongsheHuagongshe Chemistry Print Report · For research reference only
Malononitrile → (Cyclopropylhydroxy-methylene)methane-1,1-dicarbonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Malononitrile | HCID 8010 | — |
| Reactant | 3-Chlorothiophene-2-carbonyl chloride | HCID 2735824 | — |
| Reactant | [(3-Chloro(2-thienyl))hydroxymethylene]methane-1,1-dicarbonitrile | HCID 23033060 | — |
| Product | (Cyclopropylhydroxy-methylene)methane-1,1-dicarbonitrile | HCID 23122154 | — |
Reaction Steps
In a similar manner as described above, [(3-chloro(2-thienyl))hydroxymethylene]methane-1,1-dicarbonitrile was prepared from malononitrile and 3-chlorothiophene-2-carbonylchloride. The NMR data and ESI/MS data of the compound are given below.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07557113B2 |
| Source dataset | uspto-grants-2009_07 |
| ORD ID | ord-edcaea38dddf4f99aaba4abc762361e4 |
| Source note | uspto-grants-2009_07 |