HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → N-(2-Aminoethyl)-4-chlorobenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | N-(2-methylsulfonyloxyethyl)-4-chlorobenzamide | HCID 19741760 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | N-(2-Aminoethyl)-4-chlorobenzamide | HCID 4289 | — |
Reaction Steps
The N-(2-methylsulfonyloxyethyl)-4-chlorobenzamide obtained is dissolved in 5 ml of dimethylformamide and added dropwise at room temperature to a solution of ammonia in dimethylformamide. After stirring for 2 hours, the mixture is worked-up and there is obtained N-(2-aminoethyl)-4-chlorobenzamide which is identical with the product obtained in Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05238962 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-7767b183e82a4fd69c45e1964694325c |
| Source note | uspto-grants-1993_08 |