HuagongsheHuagongshe Chemistry Print Report · For research reference only
Carbon Tetrachloride → 4-(3-Chloropropyl)-2,6-dimethylmorpholine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Carbon Tetrachloride | HCID 5943 | — |
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 4-(3-Hydroxypropyl)-2,6-dimethylmorpholine | HCID 22478294 | — |
| Product | 4-(3-Chloropropyl)-2,6-dimethylmorpholine | HCID 19738017 | — |
Reaction Steps
This intermediate (2.3 g.) was prepared using the procedure described in Example 4c except using 5.0 g. (28 mmoles) of 4-(3-hydroxypropyl)-2,6-dimethylmorpholine and 9.5 g. (30 mmoles) of triphenylphosphine in 50 ml. of carbon tetrachloride and was isolated as a colorless liquid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05240925 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-4bca85dbe3a2417f979c381cad910a58 |
| Source note | uspto-grants-1993_08 |