HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 19738039, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 1-Chloromethyl-1H-1,2,4-triazole | HCID 3743882 | — |
| Reactant | HCID 53704383 | HCID 53704383 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 19738039 | HCID 19738039 | — |
Reaction Steps
This compound (400 mg.) was prepared using the procedure described in Example 2b except using 400 mg. (1.25 mmoles) of 2-(4-chlorophenyl)-6-(2,6-dimethyl-4-morpholinyl)capronitrile, 0.06 g. (1.38 mmoles) of sodium hydride, 0.15 g. (1.25 mmoles) of 1-(chloromethyl)-1,2,4-triazole, and 4 ml. of DMF and was isolated as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05240925 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-140f902fc8044903b9d45f86c4a8c1ad |
| Source note | uspto-grants-1993_08 |