HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 19738020, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Picolyl chloride hydrochloride | HCID 23392 | — |
| Reactant | (2-Methoxyphenyl)acetonitrile | HCID 81496 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 19738020 | HCID 19738020 | — |
Reaction Steps
This intermediate (80 g.) was prepared using the procedure described in Example 14a except using 50 g. (0.339 mole) of (2-methoxyphenyl)acetonitrile, 56 g. (0.339 mole) of 2-(chloromethyl)pyridine hydrochloride, 60 g. (0.746 mole) of 50% aqueous sodium hydroxide, and 200 ml. of DMSO.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05240925 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-8ee21ac7c9dd422d8c8371f897bc71ab |
| Source note | uspto-grants-1993_08 |