HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → HCID 19738086, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | 4-Isopropylpyridine | HCID 69674 | — |
| Reactant | HCID 19738095 | HCID 19738095 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 19738086 | HCID 19738086 | 87% |
Reaction Steps
N-(Phenylmethyl)-4-isopropylpyridinium chloride from 4-isopropylpyridine (129 mL, 1.0 mol), isopropanol (500 mL) and benzyl chloride (121 mL, 1.05 mol). The product was then dissolved in acetone (250 mL) and treated with sodium iodide. A precipitate formed which was collected by filtration to afford 214.6 g (87%) of N-(phenylmethyl)-4-isopropylpyridinium iodide as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05240935 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-4cee4428d110485a9a07e11b333892f4 |
| Source note | uspto-grants-1993_08 |