Triethylamine → HCID 19738262, compound

Participants

Reaction Steps

In 10 ml of dry tetrahydrofuran, 1.0 g of the 3,4-dichloro-5-isothiazolecarboxylic acid obtained in Example 2 was dissolved, followed by the dropwise addition of a solution of 0.52 g of triethylamine in 5 ml of dry tetrahydrofuran. After the resulting mixture was stirred further at room temperature for 30 minutes, the solvent was distilled off under reduced pressure so that 1.51 g (stoichiometric amount) of the title compound were obtained.

Provenance & Evidence