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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2255520Generated: November 2, 2026

Hydrochloric Acid → HCID 14668320, compound

https://huagongshe.com/reaction/2255520

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 14668318HCID 14668318—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
SolventDiethyl EtherHCID 3283—
ProductHCID 14668320HCID 14668320113.2%

Reaction Steps

A mixture of (S)-(-)-N-[(1-ethyl-2-pyrrolidinyl)methyl]-3,6-dibenzyloxy-2-methoxybenzamide (130 mg, 0.27 mmol), 5% Pd/C (50 mg), 0.5 ml 4 M HCl in ether and 5 ml ethanol was shaken in a hydrogen atmosphere for 1 h. Filtration and evaporation of the solvent gave 90 mg pure title compound as an oily hydrochloride.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05240957
Source datasetuspto-grants-1993_08
ORD IDord-bd8ff835b54c445994b2e5954daffa02
Source noteuspto-grants-1993_08