HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → HCID 19385726, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | Vanillyl alcohol | HCID 62348 | — |
| Reactant | Methyl 2-(2-bromophenyl)acetate | HCID 8063364 | — |
| Reactant | Acetone potassium carbonate | HCID 86600397 | — |
| Product | HCID 19385726 | HCID 19385726 | 25.2% |
Reaction Steps
Using the K2CO3 /acetone conditions for phenol alkylation described in Step A of Example 30, 1.00 g (6.49 mmol) of 4-hydroxy-3-methoxybenzyl alcohol was alkylated with 1.64 g (7.14 mmol) of methyl 2-bromophenylacetate to afford 0.495 g (25%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05240938 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-d926c5b806ae4eb7b4f693d83c1d5a89 |
| Source note | uspto-grants-1993_08 |