Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2818-89-5 | HCID 520368 | — |
| Reactant | Octadecyl 4-chlorobenzenesulfonate | HCID 3321883 | — |
| Product | HCID 13774191 | HCID 13774191 | 61% |
Reaction Steps
Octadecyl parachlorobenzenesulfonate (11.5 g) was added to 3.96 g of 2,5-dimethylbenzoselenazole, and the mixture was heated at 130° C. for 6 hours. The crystals yielded by the reaction were washed with ether and then recrystallized from ethyl acetate. Drying of the crystals gave 7.42 g of 2,5-dimethyl-3-octadecylbenzoselenazolium parachlorobenzenesulfonate (yield 61%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05241027 |
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| Source dataset | uspto-grants-1993_08 |
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| ORD ID | ord-063e98723f91458181f3bbd6b9bfd6c1 |
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| Source note | uspto-grants-1993_08 |
|---|
