Sarcosine → HCID 19100972, compound

HRID 2255686Notes

Reaction equation

HRID 2255686 reaction equation
[CH2:1]([N:4]([CH2:10][CH:11]=O)[C:5](=[O:9])[O:6][CH2:7][CH3:8])[CH:2]=[CH2:3].[NH:13]([CH2:15]C(O)=O)[CH3:14]>C1(C)C=CC=CC=1>[CH3:14][N:13]1[CH2:15][CH2:3][CH:2]2[CH:11]1[CH2:10][N:4]([C:5]([O:6][CH2:7][CH3:8])=[O:9])[CH2:1]2

Participants

4

Reactant 2

HCID 1088SarcosineHCID 11084330Ethyl allyl(2-oxoethyl)carbamate

Product 1

HCID 19100972HCID 19100972, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

8.6 g (50 mmol) of ethyl N-allyl-N-(2-oxoethyl)-carbamate are heated under reflux overnight with 4.5 g (50 mmol) of sarcosine in 200 ml of toluene. The mixture is concentrated and the residue is distilled.

Workup

  1. concentrationThe mixture is concentrated
  2. distillationthe residue is distilled

Sources & evidence

ORD record
ord-a402be53f3334ffa80559027f9a5b723
Source dataset
uspto-grants-1993_08
Patent number
US05241076

Reaction notes

Loading…