N-Phenylglycine → HCID 19100958, compound

HRID 2255688Notes

Reaction equation

HRID 2255688 reaction equation
[CH2:1]([N:4]([CH2:10][CH:11]=O)[C:5](=[O:9])[O:6][CH2:7][CH3:8])[CH:2]=[CH2:3].[C:13]1([NH:19][CH2:20]C(O)=O)[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>C1(C)C=CC=CC=1>[C:13]1([N:19]2[CH2:20][CH2:3][CH:2]3[CH:11]2[CH2:10][N:4]([C:5]([O:6][CH2:7][CH3:8])=[O:9])[CH2:1]3)[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1

Participants

4

Reactant 2

HCID 66025N-PhenylglycineHCID 11084330Ethyl allyl(2-oxoethyl)carbamate

Product 1

HCID 19100958HCID 19100958, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

8.6 g (50 mmol) of ethyl N-allyl-N-(2-oxoethyl)-carbamate and 7.6 g (50 mmol) of phenylglycine are heated under reflux overnight in 200 ml of toluene. The mixture is decanted from resinous material and concentrated, and the residue is distilled.

Workup

  1. customThe mixture is decanted from resinous material
  2. concentrationconcentrated
  3. distillationthe residue is distilled

Sources & evidence

ORD record
ord-79bf50925f8f4849b39e71b3ed55447c
Source dataset
uspto-grants-1993_08
Patent number
US05241076

Reaction notes

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