Water → HCID 19100966, compound

HRID 2255699Notes

Reaction equation

HRID 2255699 reaction equation
[CH2:1]([N:4]([CH:10]([CH3:13])[CH:11]=O)[C:5](=[O:9])[O:6][CH2:7][CH3:8])[CH:2]=[CH2:3].O.[NH:15]([CH2:17]C(O)=O)[CH3:16]>C1(C)C=CC=CC=1>[CH3:16][N:15]1[CH2:17][CH2:3][CH:2]2[CH:11]1[CH:10]([CH3:13])[N:4]([C:5]([O:6][CH2:7][CH3:8])=[O:9])[CH2:1]2

Participants

5

Reactant 3

HCID 962WaterHCID 1088SarcosineHCID 15069993Ethyl N-allyl-N-(1-oxoprop-2-yl)-carbamate

Product 1

HCID 19100966HCID 19100966, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

18.5 g (0.1 mol) of ethyl N-allyl-N-(1-oxoprop-2-yl)-carbamate are heated under reflux overnight in a water separator with 9 g (0.1 mol) of sarcosine in 300 ml of toluene. The mixture is concentrated and the residue is distilled.

Workup

  1. concentrationThe mixture is concentrated
  2. distillationthe residue is distilled

Sources & evidence

ORD record
ord-29bae5209e624c629b09a9973c86c00a
Source dataset
uspto-grants-1993_08
Patent number
US05241076

Reaction notes

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