HRID2255702

反应详情

EQUATION

反应方程式

HRID 2255702 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

10.3 g (50 mmol) of ethyl N-(2-chloroallyl)-N-(2-oxoethyl)-carbamate are heated under reflux overnight with 4.5 g (50 mmol) of sarcosine in 200 ml of toluene. The mixture is concentrated and the residue is distilled.

WORKUP

后处理

  1. concentrationThe mixture is concentrated
  2. distillationthe residue is distilled