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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2255708Generated: October 28, 2026

Pipecolic Acid → HCID 54122708, compound

https://huagongshe.com/reaction/2255708

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPipecolic AcidHCID 849—
ReactantEthyl allyl(2-oxoethyl)carbamateHCID 11084330—
SolventTolueneHCID 1140—
ProductHCID 54122708HCID 54122708—

Reaction Steps

17.1 g (0.1 mol) of ethyl N-allyl-N-(2-oxoethyl)-carbamate are heated under reflux overnight with 13 g (0.1 mol) of piperidine-2-carboxylic acid in 200 ml of toluene. The mixture is concentrated and the residue is distilled.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05241076
Source datasetuspto-grants-1993_08
ORD IDord-5307fd70f4944e1086f44e4f58ff79d0
Source noteuspto-grants-1993_08