Water → HCID 19100936, compound

HRID 2255713Notes

Reaction equation

HRID 2255713 reaction equation
[CH2:1]([N:4]([CH:10]([CH3:13])[CH:11]=O)[C:5](=[O:9])[O:6][CH2:7][CH3:8])[CH:2]=[CH2:3].O.[CH2:15]([NH:22][CH2:23]C(O)=O)[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1>C1(C)C=CC=CC=1>[CH2:15]([N:22]1[CH2:23][CH2:3][CH:2]2[CH:11]1[CH:10]([CH3:13])[N:4]([C:5]([O:6][CH2:7][CH3:8])=[O:9])[CH2:1]2)[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1

Participants

5

Reactant 3

HCID 962WaterHCID 869652-(Benzylamino)acetic acidHCID 15069993Ethyl N-allyl-N-(1-oxoprop-2-yl)-carbamate

Product 1

HCID 19100936HCID 19100936, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

37 g (0.2 mol) of ethyl N-allyl-N-(1-oxo-2-propyl)-carbamate are heated under reflux overnight in a water separator with 33 g (0.2 mol) of N-benzylglycine in 500 ml of toluene. The mixture is concentrated and the residue is distilled.

Workup

  1. concentrationThe mixture is concentrated
  2. distillationthe residue is distilled

Sources & evidence

ORD record
ord-846ec21827e544faabc7ef26a95e2d65
Source dataset
uspto-grants-1993_08
Patent number
US05241076

Reaction notes

Loading…