HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxygen → 3,7-Dimethylocta-2,6-Dienal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxygen | HCID 977 | — |
| Reactant | Geraniol | HCID 637566 | — |
| Reactant | Nerol | HCID 643820 | — |
| Solvent | Water | HCID 962 | — |
| Product | 3,7-Dimethylocta-2,6-Dienal | HCID 8843 | — |
Reaction Steps
The resulting catalyst precursor was reduced by passing a gaseous stream of geraniol and nerol (65% geraniol/35% nerol; 670 mg/min, 4.3 mmol/min), O2 (73 ml/min, 3.3 mmol/min), and steam (10 ml/min water) through the reactor tube at 360° C. to produce citral in 80% yield (moles of citral produced per mole of nerol/geraniol introduced; determined by capillary weight percent gas chromatograph).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05241122 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-b85cc8167169476c9983cd58e86dd25c |
| Source note | uspto-grants-1993_08 |