HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Benzyloxy) ethanol → 10-[2-(Benzyloxy)ethoxy]anthracene-9-carbaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Benzyloxy) ethanol | HCID 12141 | — |
| Reactant | 10-Chloro-9-anthraldehyde | HCID 82703 | — |
| Solvent | Methylenechloride Hexane | HCID 21226440 | — |
| Product | 10-[2-(Benzyloxy)ethoxy]anthracene-9-carbaldehyde | HCID 19738617 | 29.5% |
Reaction Steps
Using the procedure outlined in Example 2A, 10-chloroanthracene-9-carbaldehyde (Aldrich) and 2-benzyloxyethanol (Aldrich) gave a 29.5% yield of 10-[2-(benzyloxy)ethoxy]anthracene-9-carbaldehyde, mp 68°-69°, (C,H), (CH2Cl2 /hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05241107 |
| Source dataset | uspto-grants-1993_08 |
| ORD ID | ord-f2470d9bf0d741a49fcb2b5dea155c00 |
| Source note | uspto-grants-1993_08 |