HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 9945554, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Phenylbenzoyl chloride | HCID 84151 | — |
| Reactant | 5,6,7,8-Tetrahydro-4H-thieno[3,2-B]azepine | HCID 11804971 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 9945554 | HCID 9945554 | — |
Reaction Steps
As described for Example 1, a solution of 2 mmol of 5,6,7,8-tetrahydro-4H-thieno[3,2-b]azepine, 5 mmol of triethylamine and 2.1 mmol of [1,1'-biphenyl]-4-carbonyl chloride in 10 ml of CH2Cl2 is stirred at room temperature for 16 hours to give the product as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05654297 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-14f455e6a7fd4f70b797aaa404af52d4 |
| Source note | uspto-grants-1997_08 |