HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanethiol → HCID 14860709, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanethiol | HCID 6343 | — |
| Reactant | HCID 14212862 | HCID 14212862 | — |
| Reactant | HCID 14860708 | HCID 14860708 | — |
| Product | HCID 14860709 | HCID 14860709 | 38% |
Reaction Steps
Using the procedure described for the synthesis of 2-acetamido-N-benzyl-2-(methylmercapto)acetamide, 2-acetamido-N-benzyl-2-ethoxyacetamide (2.00 g, 8.0 mmol) and EtSH (0.65 g, 10.4 mmol) were converted to 0.80 g (38%) of the desired product. The compound was further purified by recrystallization from chloroform/hexane to give a beige solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05654301 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-d5803c40ece0424eade54a136ff0ad01 |
| Source note | uspto-grants-1997_08 |