HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → 1,1'-[(4-Bromo-1,3-phenylene)bis(oxymethylene)]dibenzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Bromoresorcinol | HCID 81105 | — |
| Product | 1,1'-[(4-Bromo-1,3-phenylene)bis(oxymethylene)]dibenzene | HCID 12882168 | — |
Reaction Steps
Using a procedure similar to that described in Example 17.a., except using 4-bromoresorcinol and using two equivalents of benzyl bromide and potassium carbonate, the named compound was prepared as a white solid; MS: 369; NMR: 5.0 (s, 2), 5.1(s, 2), 6.47(d, d, J1 =8, J2 =2.6, 1), 6.6 (d, J=2.7, 1), 7.2-7.5 (m, 11).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05654299 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-e45fd3c8e74148d9b187f346b072f1c6 |
| Source note | uspto-grants-1997_08 |