1-Phenethylamine, (+)- → HCID 69950762, compound

Participants

Reaction Steps

A solution of 29.7 g of 1-tert-butoxycarbonyl-3.4-epoxypyrrolidine and 41 ml of (R)-(+)-α-methylbenzylamine in 250 ml of ethanol was heated under reflux for 16 hours. The solvent was removed under reduced pressure, and a residue was subjected to silica gel column chromatography. From an eluant of a mixture of chloroform and methanol (98:2 by volume.), an oily titled compound weighing 15.3 g was obtained.

Provenance & Evidence