Phenyl isocyanate → HCID 70344828, compound

Participants

Reaction Steps

To a solution of 4-(3-aminopropyl)-2-methyl-4-phenyl-1,2,3,4-tetrahydroisoquinoline (0.4 g) in chloroform (10 ml) was added phenyl isocyanate (0.25 g) and the mixture was stirred at room temperature for 1.5 hours. The reaction mixture was concentrated to dryness and the residue was crystallized from methanol-isopropyl ether to provide the title compound (0.39 g) as colorless powder.

Provenance & Evidence