HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(3-Isopropyl-4-methoxy-phenoxy)-3,5-dimethyl-nitrobenzene → 3,5-Dimethyl4-(3'-isopropyl-4'-methoxyphenoxy)-aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(3-Isopropyl-4-methoxy-phenoxy)-3,5-dimethyl-nitrobenzene | HCID 10313602 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 3,5-Dimethyl4-(3'-isopropyl-4'-methoxyphenoxy)-aniline | HCID 10016799 | — |
Reaction Steps
3,5-Dimethyl-4-(3'-isopropyl-4'-methoxyphenoxy)-nitrobenzene (6.0 g) and 600 mg of 10% platinum on carbon in 200 ml ethanol are hydrogenated on a Parr shaker. Catalyst is removed by filtration through Celite and the filtrate is stripped to afford 3,5dimethyl-4-(3'-isopropyl-4'-methoxyphenoxy)-aniline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05654468 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-72da1e0d97e24611bff6b7e94c53b434 |
| Source note | uspto-grants-1997_08 |