Acrylonitrile → HCID 23302080, compound

HRID 2256637Notes

Reaction equation

HRID 2256637 reaction equation
[NH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][NH2:10].[C:11](#[N:14])[CH:12]=[CH2:13]>C(O)C>[C:11]([CH2:12][CH2:13][NH:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][NH:10][CH2:4][CH2:3][C:2]#[N:1])#[N:14]

Participants

4

Reactant 2

HCID 7855AcrylonitrileHCID 242501,8-Octanediamine

Product 1

HCID 23302080HCID 23302080, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Dissolve 14.4 g (0.1 mol) of 1,8-diaminooctane and 14.5 ml (0.22 mol) of acrylonitrile in 100 ml of ethanol and reflux overnight. Remove the solvent at reduced pressure. Analysis showed the title compound to be >98% pure.

Workup

  1. temperaturereflux overnight
  2. customRemove the solvent at reduced pressure

Sources & evidence

ORD record
ord-7e08d654d7c54a848825b4e79bf5e614
Source dataset
uspto-grants-1997_08
Patent number
US05654484

Reaction notes

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