3-Oxetanone → HCID 57753599, compound

HRID 225678Notes

Reaction equation

HRID 225678 reaction equation
[CH2:1]([N:8]1[CH2:16][C:15]2[C:10](=[CH:11][CH:12]=[C:13](Br)[CH:14]=2)[CH2:9]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[O:18]1[CH2:21][C:20](=[O:22])[CH2:19]1>>[CH2:1]([N:8]1[CH2:16][C:15]2[C:10](=[CH:11][CH:12]=[C:13]([C:20]3([OH:22])[CH2:21][O:18][CH2:19]3)[CH:14]=2)[CH2:9]1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 150242543-OxetanoneHCID 534165502-Benzyl-5-bromoisoindoline

Product 1

HCID 57753599HCID 57753599, compound

Procedure

Prepared in analogy to Example A62(b) from 2-benzyl-5-bromo-2,3-dihydro-1H-isoindole (Example A62(a)) and oxetan-3-one (CAS: 6704-31-0). Brown solid. MS (m/e): 282.4 ([M+H]+, 100%).

Sources & evidence

ORD record
ord-dad58ff99dd84732a6b89a7cb217f3c5
Source dataset
uspto-grants-2009_07
Patent number
US07557114B2

Reaction notes

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