HRID2256803

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID23620856

3-Hydroxy-N-methyl-L-tyrosine

C10H13NO4

结构：CN([C@@H](Cc1ccc(O)c(O)c1)C(=O)O)[C@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O

HCID131720109

未命名化合物

2 次

PRODUCTS

生成物

结构：CN[C@@H](Cc1ccc(O)c(O)c1)C(=O)O.OC[C@H]1O[C@H](O)[C@H](O)[C@@H](O)[C@@H]1O

HCID131720108

未命名化合物

PROCEDURE

实验过程

A fraction containing α-glucosyl methyldopa was recovered, concentrated in vacuo and pulverized to obtain a white α-glucosyl methyldopa preparation in the yield of about 55% against the weight of the material methyldopa, d.s.b. High-performance liquid chromatography (HPLC) analysis of the preparation revealed that it contained about 60% 3-α-glucosyl methyldopa and about 40% 4-α-glucosyl methyldopa.

WORKUP

后处理

customwas recovered
concentrationconcentrated in vacuo
customto obtain