HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 54357948, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Azepane | HCID 8119 | — |
| Reactant | HCID 22874407 | HCID 22874407 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54357948 | HCID 54357948 | 93.5% |
Reaction Steps
Benzyl(2R)-2-carboxymethyl-4-methylvalerate (1.35 g), hexahydro-1H-azepine (0.610 g) and WSCD.HCl (1.18 g) were reacted in methylene chloride (30 ml) in a similar manner to that of Preparation 1-1) to give benzyl (2R)-2-(hexahydro-1H-azepin-1-ylcarbonylmethyl)-4-methylvalerate (1.65 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05656604 |
| Source dataset | uspto-grants-1997_08 |
| ORD ID | ord-7004d01d07654fcb8cc6e459a2df236b |
| Source note | uspto-grants-1997_08 |