HRID2257097

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID24526

Chlorine

Cl2

结构：Nc1ccc(S(=O)(=O)C(F)(F)F)cc1[N+](=O)[O-]

HCID4529469

2-Nitro-4-(trifluoromethanesulfonyl)aniline

C7H5F3N2O4S

PRODUCTS

生成物

结构：Nc1c(Cl)cc(S(=O)(=O)C(F)(F)F)cc1[N+](=O)[O-]

HCID53829400

未命名化合物

收率 95.3%

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID176

Acetic Acid

C2H4O2

PROCEDURE

实验过程

Analogously to Example 14, 27 g of 2-nitro-4-trifluoromethylsulphonyl-aniline in 100 ml of acetic acid were chlorinated with 10 g of chlorine. 29 g of 2-nitro-4-trifluoromethylsulphonyl-6-chloro-aniline were obtained, melting point: 138°-139° C.