HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
1-Bromooctane → N-(6-Methylthioquinolin-5-yl)-2-octanyl-1,3-dithiane-2-carboxamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 1-Bromooctane | HCID 8140 | — |
| Edukt | 1,3-Dithiane-2-carboxylic acid | HCID 303705 | — |
| Edukt | Sodium bis(trimethylsilyl)amide | HCID 2724254 | — |
| Edukt | 5-Amino-6-methylthioquinoline | HCID 10397660 | — |
| Edukt | 2-Octanyl-1,3-dithiane-2-carboxylic acid | HCID 14995436 | — |
| Produkt | N-(6-Methylthioquinolin-5-yl)-2-octanyl-1,3-dithiane-2-carboxamide | HCID 14995437 | — |
Reaktionsschritte
5-Amino-6-methylthioquinoline, prepared as described in Example 34, was coupled with 2-octanyl-1,3-dithiane-2-carboxylic acid, prepared by treatment of 1,3-dithiane-2-carboxylic acid with sodium hexamethyldisilazide and octanyl bromide, according to Example 25 to give the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05656634 |
| Quelldatensatz | uspto-grants-1997_08 |
| ORD ID | ord-4d6c93e5e33d4516bc673bed9e497a14 |
| Quellennotiz | uspto-grants-1997_08 |